Abstract
This work demonstrates the application of a pulsed microwave system for single-step co-production of ethylene and ammonia from methane. To mitigate inherent production fluctuations from pulsed microwave reactors, a staggered manifold configuration was utilized to stabilize effluent flow for industrial-scale compatibility. Dynamic validation of the ammonia and ethylene purification columns confirmed that a rigorously tuned control strategy effectively rejects ±10% feed disturbances while maintaining process stability and product purity. Ultimately, this systematic approach establishes a robust foundation for the sustainable, electrified production of foundational chemicals by bridging the gap between laboratory-scale pulsing phenomena and industrial-scale operational reliability.