LAPSE:2020.0441
Published Article

LAPSE:2020.0441
Optimization of Sintering Parameters of 316L Stainless Steel for In-Situ Nitrogen Absorption and Surface Nitriding Using Response Surface Methodology
May 18, 2020
Abstract
This research investigates the simultaneous sintering and surface nitriding of 316L stainless steel alloy using powder metallurgy method. The influence of sintering temperature and dwell time are investigated for maximum nitrogen absorption, densification and increased microhardness using response surface methodology (RSM). In this study, 316L stainless steel powder was compacted at 800 MPa and sintered at two different temperatures of 1150 and 1200 °C with varying dwell times of 1, 3, 5 and 8 h in nitrogen atmosphere. The sintered compacts were then characterized for their microstructure, densification, microhardness and nitrogen absorption. The results revealed that increased dwell time assisted nitrogen to diffuse into stainless steel matrix along with the creation of nitride layer onto the sample surface. The microhardness and density also increased with increasing dwell time. A densification of 7.575 g/cm3 and microhardness of 235 HV were obtained for the samples sintered at 1200 °C temperature with 8 h dwell time. The simultaneous sintering and surface nitriding technique developed in this research work can help in improving corrosion resistance of this material and controlling leaching of metal ions for its potential use in biomedical applications.
This research investigates the simultaneous sintering and surface nitriding of 316L stainless steel alloy using powder metallurgy method. The influence of sintering temperature and dwell time are investigated for maximum nitrogen absorption, densification and increased microhardness using response surface methodology (RSM). In this study, 316L stainless steel powder was compacted at 800 MPa and sintered at two different temperatures of 1150 and 1200 °C with varying dwell times of 1, 3, 5 and 8 h in nitrogen atmosphere. The sintered compacts were then characterized for their microstructure, densification, microhardness and nitrogen absorption. The results revealed that increased dwell time assisted nitrogen to diffuse into stainless steel matrix along with the creation of nitride layer onto the sample surface. The microhardness and density also increased with increasing dwell time. A densification of 7.575 g/cm3 and microhardness of 235 HV were obtained for the samples sintered at 1200 °C temperature with 8 h dwell time. The simultaneous sintering and surface nitriding technique developed in this research work can help in improving corrosion resistance of this material and controlling leaching of metal ions for its potential use in biomedical applications.
Record ID
Keywords
316L stainless steel, nitrogen absorption, response surface methodology, sintering, surface nitriding
Subject
Suggested Citation
Ali S, Abdul Rani AM, Ahmad Mufti R, Ahmed SW, Baig Z, Hastuty S, Razak MAA, Abdu Aliyu AA. Optimization of Sintering Parameters of 316L Stainless Steel for In-Situ Nitrogen Absorption and Surface Nitriding Using Response Surface Methodology. (2020). LAPSE:2020.0441
Author Affiliations
Ali S: School of Mechanical & Manufacturing Engineering, National University of Sciences and Technology (NUST), H-12, Islamabad 44000, Pakistan [ORCID]
Abdul Rani AM: Mechanical Engineering Department, Universiti Teknologi PETRONAS (UTP), Seri Iskandar 32610, Malaysia
Ahmad Mufti R: School of Mechanical & Manufacturing Engineering, National University of Sciences and Technology (NUST), H-12, Islamabad 44000, Pakistan
Ahmed SW: Department of Mechanical Engineering, Ghulam Ishaq Khan Institute of Engineering Sciences and Technology, Khyber Pakhtunkhwa 19201, Pakistan
Baig Z: Centre of Excellence in Science & Applied Technologies, Islamabad 44000, Pakistan
Hastuty S: Mechanical Engineering Department, Universitas PERTAMINA, Jakarta 12220, Indonesia
Razak MAA: Manufacturing Section, Universiti Kuala Lumpur Malaysian Spanish Institute, Kulim Hi-Tech Park, Kedah 09000, Malaysia [ORCID]
Abdu Aliyu AA: Mechanical Engineering Department, Bayero University Kano, Kano 700241, Nigeria
Abdul Rani AM: Mechanical Engineering Department, Universiti Teknologi PETRONAS (UTP), Seri Iskandar 32610, Malaysia
Ahmad Mufti R: School of Mechanical & Manufacturing Engineering, National University of Sciences and Technology (NUST), H-12, Islamabad 44000, Pakistan
Ahmed SW: Department of Mechanical Engineering, Ghulam Ishaq Khan Institute of Engineering Sciences and Technology, Khyber Pakhtunkhwa 19201, Pakistan
Baig Z: Centre of Excellence in Science & Applied Technologies, Islamabad 44000, Pakistan
Hastuty S: Mechanical Engineering Department, Universitas PERTAMINA, Jakarta 12220, Indonesia
Razak MAA: Manufacturing Section, Universiti Kuala Lumpur Malaysian Spanish Institute, Kulim Hi-Tech Park, Kedah 09000, Malaysia [ORCID]
Abdu Aliyu AA: Mechanical Engineering Department, Bayero University Kano, Kano 700241, Nigeria
Journal Name
Processes
Volume
8
Issue
3
Article Number
E297
Year
2020
Publication Date
2020-03-05
ISSN
2227-9717
Version Comments
Original Submission
Other Meta
PII: pr8030297, Publication Type: Journal Article
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LAPSE:2020.0441
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https://doi.org/10.3390/pr8030297
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[v1] (Original Submission)
May 18, 2020
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May 18, 2020
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Calvin Tsay
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