LAPSE:2023.1101
Published Article

LAPSE:2023.1101
Omega Phase Formation and Mechanical Properties of Ti−1.5 wt.% Mo and Ti−15 wt.% Mo Alloys after High-Pressure Torsion
February 21, 2023
Abstract
The paper analyzes the effect of severe plastic deformation by the high-pressure torsion (HPT) on phase transformations, in particular, on the formation of the ω-phase, and on mechanical properties, such as hardness and Young’s modulus, in Ti alloys with 1.5 and 15 wt.% Mo. Both alloys were pre-annealed at 1000 °C for 24 h and quenched. The microstructure of the initial Ti−1.5 wt.% Mo alloy consisted of the α-phase and α’-martensite, and the initial Ti−15 wt.% Mo alloy contained polycrystalline β solid solution. The hardness tests of the samples were carried out under the load of 10 and 200 mN. The annealed alloys were subjected to HPT, and the micro- and nanohardness of both deformed samples increased up to ~1 GPa compared to their initial state. It turned out that the values of hardness (H) and Young’s modulus (E) depend on the applied load on the indenter: the higher the applied load, the lower H and higher E. It was also found that the HPT leads to the 30% increase in E for an alloy with 1.5 wt.% Mo and to the 9% decrease in E for the alloy with 15 wt.% Mo. Such a difference in the behavior of the Young’s modulus is associated with phase transformations caused by the HPT.
The paper analyzes the effect of severe plastic deformation by the high-pressure torsion (HPT) on phase transformations, in particular, on the formation of the ω-phase, and on mechanical properties, such as hardness and Young’s modulus, in Ti alloys with 1.5 and 15 wt.% Mo. Both alloys were pre-annealed at 1000 °C for 24 h and quenched. The microstructure of the initial Ti−1.5 wt.% Mo alloy consisted of the α-phase and α’-martensite, and the initial Ti−15 wt.% Mo alloy contained polycrystalline β solid solution. The hardness tests of the samples were carried out under the load of 10 and 200 mN. The annealed alloys were subjected to HPT, and the micro- and nanohardness of both deformed samples increased up to ~1 GPa compared to their initial state. It turned out that the values of hardness (H) and Young’s modulus (E) depend on the applied load on the indenter: the higher the applied load, the lower H and higher E. It was also found that the HPT leads to the 30% increase in E for an alloy with 1.5 wt.% Mo and to the 9% decrease in E for the alloy with 15 wt.% Mo. Such a difference in the behavior of the Young’s modulus is associated with phase transformations caused by the HPT.
Record ID
Keywords
hardness, high-pressure torsion, nanoindentation, pre-annealing, titanium alloys, Young’s modulus
Subject
Suggested Citation
Gornakova AS, Korneva A, Tyurin AI, Afonikova NS, Kilmametov AR, Straumal BB. Omega Phase Formation and Mechanical Properties of Ti−1.5 wt.% Mo and Ti−15 wt.% Mo Alloys after High-Pressure Torsion. (2023). LAPSE:2023.1101
Author Affiliations
Gornakova AS: Osipyan Institute of Solid State Physics of the Russian Academy of Sciences, Ac. Osipyan Str. 2, 142432 Chernogolovka, Russia
Korneva A: Institute of Metallurgy and Materials Science Polish Academy of Sciences, Reymonta Str. 25, 30-059 Cracow, Poland [ORCID]
Tyurin AI: G.R. Derzhavin Research Institute “Nanotechnologies and Nanomaterials” TSU, Internazionalnaja Str. 30, 392000 Tambov, Russia
Afonikova NS: Osipyan Institute of Solid State Physics of the Russian Academy of Sciences, Ac. Osipyan Str. 2, 142432 Chernogolovka, Russia
Kilmametov AR: Osipyan Institute of Solid State Physics of the Russian Academy of Sciences, Ac. Osipyan Str. 2, 142432 Chernogolovka, Russia
Straumal BB: Osipyan Institute of Solid State Physics of the Russian Academy of Sciences, Ac. Osipyan Str. 2, 142432 Chernogolovka, Russia
Korneva A: Institute of Metallurgy and Materials Science Polish Academy of Sciences, Reymonta Str. 25, 30-059 Cracow, Poland [ORCID]
Tyurin AI: G.R. Derzhavin Research Institute “Nanotechnologies and Nanomaterials” TSU, Internazionalnaja Str. 30, 392000 Tambov, Russia
Afonikova NS: Osipyan Institute of Solid State Physics of the Russian Academy of Sciences, Ac. Osipyan Str. 2, 142432 Chernogolovka, Russia
Kilmametov AR: Osipyan Institute of Solid State Physics of the Russian Academy of Sciences, Ac. Osipyan Str. 2, 142432 Chernogolovka, Russia
Straumal BB: Osipyan Institute of Solid State Physics of the Russian Academy of Sciences, Ac. Osipyan Str. 2, 142432 Chernogolovka, Russia
Journal Name
Processes
Volume
11
Issue
1
First Page
221
Year
2023
Publication Date
2023-01-10
ISSN
2227-9717
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Original Submission
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PII: pr11010221, Publication Type: Journal Article
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LAPSE:2023.1101
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https://doi.org/10.3390/pr11010221
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