LAPSE:2020.0966
Published Article
LAPSE:2020.0966
Covalently Cross-Linked Nanoparticles Based on Ferulated Arabinoxylans Recovered from a Distiller’s Dried Grains Byproduct
September 15, 2020
The purpose of this investigation was to extract ferulated arabinoxylans (AX) from dried distillers’ grains with solubles (DDGS) plus to investigate their capability to form covalently cross-linked nanoparticles. AX registered 7.3 µg of ferulic acid/mg polysaccharide and molecular weight and intrinsic viscosity of 661 kDa and 149 mL/g, correspondingly. Fourier transform infrared spectroscopy (FTIR) was used to confirm the identity of this polysaccharide. AX formed laccase induced covalent gels at 1% (w/v), which registered an elastic modulus of 224 Pa and a content of FA dimers of 1.5 µg/mg polysaccharide. Scanning electron microscopy pictures of AX gels exhibited a microstructure resembling a rough honeycomb. AX formed covalently cross-linked nanoparticles (NAX) by coaxial electrospray. The average hydrodynamic diameter of NAX determined by dynamic light scattering was 328 nm. NAX presented a spherical and regular shape by transmission electron microscopy analysis. NAX may be an attractive material for pharmaceutical and biomedical applications and an option in sustainable DDGS use.
Keywords
bioethanol industry, cross-linking, electrospray, ferulated arabinoxylans, nanoparticles
Suggested Citation
De Anda-Flores Y, Carvajal-Millan E, Lizardi-Mendoza J, Rascon-Chu A, Martínez-López AL, Marquez-Escalante J, Brown-Bojorquez F, Tanori-Cordova J. Covalently Cross-Linked Nanoparticles Based on Ferulated Arabinoxylans Recovered from a Distiller’s Dried Grains Byproduct. (2020). LAPSE:2020.0966
Author Affiliations
De Anda-Flores Y: Biopolymers-CTAOA, Research Center for Food and Development (CIAD, A.C.), Carretera Gustavo Enrique Astiazaran Rosas No. 46, Hermosillo 83304, Sonora, Mexico [ORCID]
Carvajal-Millan E: Biopolymers-CTAOA, Research Center for Food and Development (CIAD, A.C.), Carretera Gustavo Enrique Astiazaran Rosas No. 46, Hermosillo 83304, Sonora, Mexico [ORCID]
Lizardi-Mendoza J: Biopolymers-CTAOA, Research Center for Food and Development (CIAD, A.C.), Carretera Gustavo Enrique Astiazaran Rosas No. 46, Hermosillo 83304, Sonora, Mexico [ORCID]
Rascon-Chu A: Biotechnology-CTAOV, Research Center for Food and Development (CIAD, A.C.), Carretera Gustavo Enrique Astiazaran Rosas No. 46, Hermosillo 83304, Sonora, Mexico [ORCID]
Martínez-López AL: NANO-VAC Research Group, Department of Chemistry and Pharmaceutical Technology, University of Navarra, 31008 Pamplona, Spain [ORCID]
Marquez-Escalante J: Biopolymers-CTAOA, Research Center for Food and Development (CIAD, A.C.), Carretera Gustavo Enrique Astiazaran Rosas No. 46, Hermosillo 83304, Sonora, Mexico [ORCID]
Brown-Bojorquez F: Department of Polymers and Materials Research, University of Sonora, Hermosillo 83000, Sonora, Mexico
Tanori-Cordova J: Department of Polymers and Materials Research, University of Sonora, Hermosillo 83000, Sonora, Mexico
Journal Name
Processes
Volume
8
Issue
6
Article Number
E691
Year
2020
Publication Date
2020-06-13
Published Version
ISSN
2227-9717
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Original Submission
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PII: pr8060691, Publication Type: Journal Article
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LAPSE:2020.0966
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doi:10.3390/pr8060691
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Sep 15, 2020
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Calvin Tsay
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